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開始行:
[[S1249 Phase-3]]
#attach
*Reports [#wa7fd940]
- Oct. 11, 2012 Okada : Aerogel target with a sub-structure of 100um scale &ref(./20121011_aerogel_target_with_a_sub-structure_of_100um_scale.pdf);
- Oct. 30, 2012 Fujiwara : Aerogel SEM and TEM image &ref(./20121030.pdf); &ref(./20121030.key);
- Nov. 11, 2012 Okada : Typical SEM and TEM images of Aerogel @ RIKEN &ref(./20121101_ImagesOfAerogel.pdf);
- Nov. 21, 2012 Okada : Aerogel TEM images &ref(./20121121_AerogelTEMImages.pdf);
- Dec. 05, 2012 Okada : Aerogel SEM images &ref(./20121205_AerogelSEMImages.pdf);
- Feb. 08, 2013 Okada : about AFM &ref(./20130208_AFM.pdf);
- Mar. 14, 2013 Okada : TEM images of low-transparent aerogels &ref(./20130314_TEM.pdf);
* SEM images [#yf715b5e]
- Oct. 16, 2012 : improvement of sampling technique (50mg/cc & 180mg/cc aerogels) &ref(./0.049と0.18 .docx);
-- 粉砕するのではなくナイフで切り出した。5mm角＊厚さ3mm。Pt-Pd蒸着1nm程度。撮影した面は、切断によって新たに生まれた表面。カーボンペーストがかかっている領域・かかっていない領域を撮影。カーボンペーストがかかった領域では粒径が大きくなるように見える→これまでのAerogel写真は撮影に失敗していた。
- Oct. 29, 2012 : comparison with Tabata-san's SEM images for 0.011g/cc sample
-- images taken at RIKEN (Os coating (2~8nm) and Os staining) :
&ref(20121029 0.011g／cm3 Osコーティング.pdf);
--- commnets for Fig.1-1 - Fig.1-20 (Os coating) : [[Note1]]
--- comments for Fig.1-21 - end (Os staining + Os coating) : [[Note2]]
-- images taken by Tabata-san : Os coating (1.5nm) :
&ref(img-7191016-0001-3.pdf);
&ref(img-7191016-0001-1-2.pdf);
- Nov. 16, 2012 : SEM test image (Os coating (5nm) & Os staining) for 50 mg/cc aerogel &ref(./20121029OsCoat5nmOsEvap2h.zip);
-- commnets : 表面か内部かの判別は出来ない．サンプルサイズ〜1.5mm角．
- Dec. 05, 2012 : SEM images for all densities &ref(20121205_SEM_AllSample_doc.zip); &ref(20121205_SEM_AllSample_pdf.zip); &ref(20121220_SEM_AllSample_raw.zip);
* TEM images [#bfe0dff8]
- Oct. 30, 2012 : test TEM images for 47 mg/cc &ref(./TEM_121029.zip);(20121030)&br;
- Nov. 09, 2012 : TEM images for all densities [[ALL SAMPLE]]
* SHIM images [#i406f7c2]
- Jun. 11, 2013 : images of Scanning Helium Ion Microscope at NIMS for 100mg/cc aerogel (MSR2-3a) &ref(./20130611_SHIM.zip);&br;
終了行:
[[S1249 Phase-3]]
#attach
*Reports [#wa7fd940]
- Oct. 11, 2012 Okada : Aerogel target with a sub-structure of 100um scale &ref(./20121011_aerogel_target_with_a_sub-structure_of_100um_scale.pdf);
- Oct. 30, 2012 Fujiwara : Aerogel SEM and TEM image &ref(./20121030.pdf); &ref(./20121030.key);
- Nov. 11, 2012 Okada : Typical SEM and TEM images of Aerogel @ RIKEN &ref(./20121101_ImagesOfAerogel.pdf);
- Nov. 21, 2012 Okada : Aerogel TEM images &ref(./20121121_AerogelTEMImages.pdf);
- Dec. 05, 2012 Okada : Aerogel SEM images &ref(./20121205_AerogelSEMImages.pdf);
- Feb. 08, 2013 Okada : about AFM &ref(./20130208_AFM.pdf);
- Mar. 14, 2013 Okada : TEM images of low-transparent aerogels &ref(./20130314_TEM.pdf);
* SEM images [#yf715b5e]
- Oct. 16, 2012 : improvement of sampling technique (50mg/cc & 180mg/cc aerogels) &ref(./0.049と0.18 .docx);
-- 粉砕するのではなくナイフで切り出した。5mm角＊厚さ3mm。Pt-Pd蒸着1nm程度。撮影した面は、切断によって新たに生まれた表面。カーボンペーストがかかっている領域・かかっていない領域を撮影。カーボンペーストがかかった領域では粒径が大きくなるように見える→これまでのAerogel写真は撮影に失敗していた。
- Oct. 29, 2012 : comparison with Tabata-san's SEM images for 0.011g/cc sample
-- images taken at RIKEN (Os coating (2~8nm) and Os staining) :
&ref(20121029 0.011g／cm3 Osコーティング.pdf);
--- commnets for Fig.1-1 - Fig.1-20 (Os coating) : [[Note1]]
--- comments for Fig.1-21 - end (Os staining + Os coating) : [[Note2]]
-- images taken by Tabata-san : Os coating (1.5nm) :
&ref(img-7191016-0001-3.pdf);
&ref(img-7191016-0001-1-2.pdf);
- Nov. 16, 2012 : SEM test image (Os coating (5nm) & Os staining) for 50 mg/cc aerogel &ref(./20121029OsCoat5nmOsEvap2h.zip);
-- commnets : 表面か内部かの判別は出来ない．サンプルサイズ〜1.5mm角．
- Dec. 05, 2012 : SEM images for all densities &ref(20121205_SEM_AllSample_doc.zip); &ref(20121205_SEM_AllSample_pdf.zip); &ref(20121220_SEM_AllSample_raw.zip);
* TEM images [#bfe0dff8]
- Oct. 30, 2012 : test TEM images for 47 mg/cc &ref(./TEM_121029.zip);(20121030)&br;
- Nov. 09, 2012 : TEM images for all densities [[ALL SAMPLE]]
* SHIM images [#i406f7c2]
- Jun. 11, 2013 : images of Scanning Helium Ion Microscope at NIMS for 100mg/cc aerogel (MSR2-3a) &ref(./20130611_SHIM.zip);&br;
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